C₂₆H₂₈IN₅O₄

Base Information

Chemical Name:C₂₆H₂₈IN₅O₄
CAS No.:1314136-95-2
Molecular Formula:C₂₆H₂₈IN₅O₄
Molecular Weight:601.444
Hs Code.:

C<sub>26</sub>H<sub>28</sub>IN<sub>5</sub>O<sub>4</sub>

Synonyms:C₂₆H₂₈IN₅O₄

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Chemical Property of C₂₆H₂₈IN₅O₄

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Technology Process of C₂₆H₂₈IN₅O₄

There total 6 articles about C₂₆H₂₈IN₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1314136-94-1
C₂₆H₂₉N₅O₄

: 1314136-95-2
C₂₆H₂₈IN₅O₄

Guidance literature:: With copper(l) iodide; N-iodomorpholine-hydrogen iodide; In tetrahydrofuran; at 20 ℃; Molecular sieve;
DOI:10.1021/ol201567s

Reference yield:

: 1314136-91-8
C₂₀H₂₁NO₄

: 1314136-95-2
C₂₆H₂₈IN₅O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 20 °C

1.2: 20 °C

2.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 20 °C

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: copper(l) iodide; N-iodomorpholine-hydrogen iodide / tetrahydrofuran / 20 °C / Molecular sieve

With copper(l) iodide; lithium hydroxide monohydrate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-iodomorpholine-hydrogen iodide; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ol201567s

Reference yield:

: 1314136-92-9
C₂₃H₂₃NO₄

: 1314136-95-2
C₂₆H₂₈IN₅O₄

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 20 °C

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: copper(l) iodide; N-iodomorpholine-hydrogen iodide / tetrahydrofuran / 20 °C / Molecular sieve

With copper(l) iodide; lithium hydroxide monohydrate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-iodomorpholine-hydrogen iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ol201567s