tris(benzoinoximato)iron(III)

Base Information

Chemical Name:tris(benzoinoximato)iron(III)
CAS No.:934348-63-7
Molecular Formula:C₄₂H₃₆FeN₃O₆
Molecular Weight:734.611
Hs Code.:

Synonyms:tris(benzoinoximato)iron(III)

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Chemical Property of tris(benzoinoximato)iron(III)

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Technology Process of tris(benzoinoximato)iron(III)

There total 1 articles about tris(benzoinoximato)iron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 121714-78-1,24290-40-2,58694-80-7,10025-77-1,64333-00-2
iron(III) chloride hexahydrate

: 441-38-3
benzoin oxime

: 934348-63-7
tris(benzoinoximato)iron(III)

Guidance literature:: With Et₃N; In ethanol; Et3N was added dropwise to EtOH soln. of the oxime-compd. at room temp. under stirring, stoich. amt. of Fe-salt soln. in EtOH was added, heatingat 70 °C for 18 h; residue was sepd., washed with cold EtOH, dried, dissolved in CH2Cl2, chromy. (neutral alumina, CH2Cl2-ether (9:1, v/v)), slow evapn. in Ar flow, drying in vac. overnight, elem. anal.;
DOI:10.1016/j.poly.2006.09.029

Reference yield: 64.0%

: 934348-63-7
tris(benzoinoximato)iron(III)

: potassium hydroxide

: μ-dihydroxy(bis(bis(benzoinoximato)iron(III)))

Guidance literature:: In methanol; acetonitrile; byproducts: potassium salt of α-benzoinoxime; MeOH soln. of KOH was added to MeCN soln. of Fe-salt, stirring for 36 h; drying in vac., washing with hot 95 % EtOH, redissoln. in CH2Cl2, chromy. (silica, CH2Cl2-ether, 80:20, v/v), slow evapn. in Ar flow, drying in vac. overnight, elem. anal.;
DOI:10.1016/j.poly.2006.09.029