C₂₅H₂₄FNO₄S

Base Information

Chemical Name:C₂₅H₂₄FNO₄S
CAS No.:1318251-60-3
Molecular Formula:C₂₅H₂₄FNO₄S
Molecular Weight:453.534
Hs Code.:

C<sub>25</sub>H<sub>24</sub>FNO<sub>4</sub>S

Synonyms:C₂₅H₂₄FNO₄S

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Chemical Property of C₂₅H₂₄FNO₄S

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Technology Process of C₂₅H₂₄FNO₄S

There total 7 articles about C₂₅H₂₄FNO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1318251-59-0
C₁₈H₁₈FNO₂

: 98-59-9
p-toluenesulfonyl chloride

: 1318251-60-3
C₂₅H₂₄FNO₄S

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1016/j.tetlet.2011.05.120

Reference yield:

: 1318251-56-7
C₂₀H₂₁NO₂S

: 1318251-60-3
C₂₅H₂₄FNO₄S

Guidance literature:: Multi-step reaction with 4 steps

1: isopropyl alcohol / 80 °C

2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / ethanol / Reflux

3: bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate / 1,2-dimethoxyethane; water

4: pyridine / dichloromethane

With pyridine; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydrogencarbonate; isopropyl alcohol; In 1,2-dimethoxyethane; ethanol; dichloromethane; water; 3: Suzuki coupling;
DOI:10.1016/j.tetlet.2011.05.120

Reference yield:

: thiophene-3-carboxylic acid (2-bromo-phenyl)-methyl-amide

: 1318251-60-3
C₂₅H₂₄FNO₄S

Guidance literature:: Multi-step reaction with 6 steps

1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 110 °C

2: toluene-4-sulfonic acid / toluene / 20 °C

3: isopropyl alcohol / 80 °C

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / ethanol / Reflux

5: bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate / 1,2-dimethoxyethane; water

6: pyridine / dichloromethane

With pyridine; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; isopropyl alcohol; In 1,2-dimethoxyethane; ethanol; dichloromethane; water; toluene; 5: Suzuki coupling;
DOI:10.1016/j.tetlet.2011.05.120