C₄₁H₄₅F₃N₂O₁₁S₂Si

Base Information

Chemical Name:C₄₁H₄₅F₃N₂O₁₁S₂Si
CAS No.:1352230-33-1
Molecular Formula:C₄₁H₄₅F₃N₂O₁₁S₂Si
Molecular Weight:891.028
Hs Code.:

C<sub>41</sub>H<sub>45</sub>F<sub>3</sub>N<sub>2</sub>O<sub>11</sub>S<sub>2</sub>Si

Synonyms:C₄₁H₄₅F₃N₂O₁₁S₂Si

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Chemical Property of C₄₁H₄₅F₃N₂O₁₁S₂Si

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Technology Process of C₄₁H₄₅F₃N₂O₁₁S₂Si

There total 14 articles about C₄₁H₄₅F₃N₂O₁₁S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1057385-93-9
(3aR,5S,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5-carbaldehyde

: 1352230-33-1
C₄₁H₄₅F₃N₂O₁₁S₂Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.2: 1 h / -78 - 20 °C

4.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

4.2: 3 h / -78 °C

4.3: 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.2: 1 h / -78 - 20 °C

6.1: lithium borohydride; methanol / tetrahydrofuran / 2 h / -78 °C

7.1: sulfuric acid / 2 h / 20 °C

8.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

8.2: 0 - 60 °C

9.1: potassium carbonate; methanol

10.1: pyridine

11.1: pyridine / 5.5 h / 0 - 20 °C

With pyridine; methanol; lithium borohydride; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; water; potassium carbonate; dimethyl sulfoxide; triethylamine; sodium hydroxide; sulfuric acid; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 3-O-(naphthalene-2-ylmethyl)-1,2;5,6-0-di(isopropylidene)-α-D-allofuranose

: 1352230-33-1
C₄₁H₄₅F₃N₂O₁₁S₂Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.2: 1 h / -78 - 20 °C

6.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

6.2: 3 h / -78 °C

6.3: 20 °C

7.1: sulfuric acid / 2 h / 20 °C

8.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

8.2: 0 - 60 °C

9.1: potassium carbonate / methanol / 96 h / 20 °C

9.2: 12 h / 0 °C

10.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

10.2: 1.5 h

11.1: pyridine / 5.5 h / 0 - 20 °C

With pyridine; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; water; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; sodium hydroxide; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 620630-82-2
1,2 5,6-O-di(isopropylidene)-α-D-allofuranose

: 1352230-33-1
C₄₁H₄₅F₃N₂O₁₁S₂Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 1 h / -78 - 20 °C

7.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

7.2: 3 h / -78 °C

7.3: 20 °C

8.1: sulfuric acid / 2 h / 20 °C

9.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

9.2: 0 - 60 °C

10.1: potassium carbonate / methanol / 96 h / 20 °C

10.2: 12 h / 0 °C

11.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

11.2: 1.5 h

12.1: pyridine / 5.5 h / 0 - 20 °C

With pyridine; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; water; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; sodium hydroxide; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;