2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester

Base Information

Chemical Name:2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester
CAS No.:686718-73-0
Molecular Formula:C₁₇H₂₄FNO₃S
Molecular Weight:341.447
Hs Code.:

Synonyms:2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester

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Chemical Property of 2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester

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Technology Process of 2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester

There total 1 articles about 2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.2%

: 107-03-9
1-thiopropane

: 114873-01-7,114873-11-9
N-Boc-3-fluoro-L-phenylalanine

: 686718-73-0
2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester

Guidance literature:: N-Boc-3-fluoro-L-phenylalanine; With triethylamine; isobutyl chloroformate; In dichloromethane; at -10 - -5 ℃;

1-thiopropane; In dichloromethane; at -5 - 0 ℃; Further stages.;
DOI:10.1016/j.tetlet.2004.07.097

Reference yield: 67.0%

: 193065-68-8
(3-ethoxy-3-oxopropyl)zinc(II) bromide

: 686718-73-0
2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester

: 686718-74-1
5-tert-butoxycarbonylamino-L-6-(3-fluorophenyl)-4-oxo-hexanoic acid ethyl ester

Guidance literature:: With phthalic anhydride; dichlorobis(triethylphosphine)palladium(II); In tetrahydrofuran;
DOI:10.1016/j.tetlet.2004.07.097

Reference yield: 54.0%

: 27374-25-0
[(1-Ethoxycyclopropyl)oxy]trimethylsilane

: 686718-73-0
2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester

: 686718-74-1
5-tert-butoxycarbonylamino-L-6-(3-fluorophenyl)-4-oxo-hexanoic acid ethyl ester

Guidance literature:: [(1-Ethoxycyclopropyl)oxy]trimethylsilane; With zinc(II) chloride; In tetrahydrofuran;

2-tert-butoxycarbonylamino-L-3-(3-fluorophenyl)-thiopropionic acid S-propyl ester; With phthalic anhydride; bis(triethylphosphine)nickel(II) chloride; In N,N-dimethyl acetamide; Further stages.;
DOI:10.1016/j.tetlet.2004.07.097