(1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate

Base Information

Chemical Name:(1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate
CAS No.:157261-83-1
Molecular Formula:C₂₄H₂₀B*C₃₂H₅₃FeP₂
Molecular Weight:874.801
Hs Code.:

Synonyms:(1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate

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Chemical Property of (1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate

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Technology Process of (1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate

There total 1 articles about (1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 157261-67-1
[chloro(1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)iron]

: 143-66-8
sodium tetraphenyl borate

: 4440-01-1
lithium phenylacetylide

: 157261-83-1
(1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate

Guidance literature:: With HBF₄*Et₂O; In tetrahydrofuran; under N2; LiCCPh in THF is added to a soln. of the starting complex in THF, mixt. stirred at room temp. for 30 min., solvent removed in vac., residue extd., filtd., HBF4*Et2O is added, soln. taken to dryness, solid dissolved in EtOH, NaBPh4 is added; the ppt. is filtd., washed, dried in vac., recrystd.; elem. anal.;
DOI:10.1021/om00020a052

Reference yield: 73.0%

: 157261-83-1
(1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCHPh)iron tetraphenylborate

: (1,2-bis(diisopropylphosphino)ethane)(pentamethylcyclopentadienyl)(CCPh)iron tetraphenylborate

Guidance literature:: With KOtBu; In tetrahydrofuran; under N2; stirred at room temp. for 1 h; the solvent is removed under vac., the residue is extd., fitd., concd.,cooled to -20°C; elem. anal.;
DOI:10.1021/om00020a052