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(E)-O-cinnamyl butylcarbamothioate

Base Information
  • Chemical Name:(E)-O-cinnamyl butylcarbamothioate
  • CAS No.:1228453-80-2
  • Molecular Formula:C14H19NOS
  • Molecular Weight:249.377
  • Hs Code.:
(E)-O-cinnamyl butylcarbamothioate

Synonyms:(E)-O-cinnamyl butylcarbamothioate

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Chemical Property of (E)-O-cinnamyl butylcarbamothioate
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Technology Process of (E)-O-cinnamyl butylcarbamothioate

There total 1 articles about (E)-O-cinnamyl butylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
(2E)-3-phenyl-2-propen-1-ol; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
butyl isothiocyanate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo1006152
Guidance literature:
With propylamine; O,O'-(S)-(1,1'-dinaphthyl-2,2'-diyl)-N,N-di-(S,S)-[2-phenylethylphosphoramidite]; bis(1,5-cyclooctadiene)diiridium(I) dichloride; potassium acetate; In 1,4-dioxane; at 50 ℃; optical yield given as %ee; enantiospecific reaction; Inert atmosphere;
DOI:10.1021/jo1006152
Guidance literature:
With propylamine; O,O'-(S)-(1,1'-dinaphthyl-2,2'-diyl)-N,N-di-(S,S)-[2-phenylethylphosphoramidite]; bis(1,5-cyclooctadiene)diiridium(I) dichloride; potassium acetate; In dichloromethane; at 50 ℃; for 12h; optical yield given as %ee; enantiospecific reaction; Inert atmosphere;
DOI:10.1021/jo1006152
upstream raw materials:

butyl isothiocyanate

(2E)-3-phenyl-2-propen-1-ol

Downstream raw materials:

C14H19NOS

C15H21NOS

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