2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile

Base Information

• Chemical Name: 2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile
• CAS No.: 72141-37-8
• Molecular Formula: C₂₂H₂₃N₃OS
• Molecular Weight: 377.51
• Mol file: 72141-37-8.mol

Synonyms:2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile

Chemical Property of 2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile

There total 5 articles about 2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-imidazol-1-ylmethyl-2-(4-phenylsulfanyl-phenyl)-hexanenitrile (72141-35-6) → 2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile (72141-37-8)

Guidance literature:

With conc. nitric acid; m-chloroperoxybenzoic acid; In dichloromethane;

Reference yield:

2-Cyano-2-(4-phenylthiophenyl)hexyl bromide → 2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile (72141-37-8)

Guidance literature:

Multi-step reaction with 2 steps

2: conc. nitric acid; m-chloroperoxybenzoic acid / dichloromethane

With conc. nitric acid; m-chloroperoxybenzoic acid; In dichloromethane;

Reference yield:

1-cyanomethyl-4-phenylthiobenzene (6317-59-5) → 2-(4-benzenesulfinyl-phenyl)-2-imidazol-1-ylmethyl-hexanenitrile (72141-37-8)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydroxide; tetraethylammonium bromide

2: sodium hydroxide; dimethyl sulfoxide

4: conc. nitric acid; m-chloroperoxybenzoic acid / dichloromethane

With sodium hydroxide; conc. nitric acid; m-chloroperoxybenzoic acid; tetraethylammonium bromide; dimethyl sulfoxide; In dichloromethane;

upstream raw materials:

2-imidazol-1-ylmethyl-2-(4-phenylsulfanyl-phenyl)-hexanenitrile

1-cyanomethyl-4-phenylthiobenzene