1-cyclohexylvinyl benzoate

Base Information

Chemical Name:1-cyclohexylvinyl benzoate
CAS No.:1256152-01-8
Molecular Formula:C₁₅H₁₈O₂
Molecular Weight:230.307
Hs Code.:

Synonyms:1-cyclohexylvinyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-cyclohexylvinyl benzoate

Chemical Property:

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Technology Process of 1-cyclohexylvinyl benzoate

There total 2 articles about 1-cyclohexylvinyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 931-48-6
2-cyclohexylacetylene

: 65-85-0,8013-63-6
benzoic acid

: 1256152-01-8
1-cyclohexylvinyl benzoate

Guidance literature:: With trans-[RuCl2(η3:η3-2,7-dimethylocta-2,6-diene-1,8-diyl)(PPh3)]; In water; at 60 ℃; for 3h; regioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/om1010325

Reference yield:

: 931-48-6
2-cyclohexylacetylene

: 65-85-0,8013-63-6
benzoic acid

: 1256151-88-8
(Z)-2-cyclohexylvinyl benzoate

: 1256152-01-8
1-cyclohexylvinyl benzoate

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 2-diphenylphosphinomethylpyridine; In tetrahydrofuran; at 110 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol102365e

Reference yield:

: 1256152-01-8
1-cyclohexylvinyl benzoate

: 153729-88-5
(1R)-1-cyclohexylethyl benzoate

: (S)-1-cyclohexylethyl benzoate

Guidance literature:: With C₃₈H₄₆O₃P₂*C₇H₈*Rh⁽¹⁺⁾*BF₄^(1-); hydrogen; In dichloromethane; at 40 ℃; for 24h; under 3000.3 Torr; Reagent/catalyst; Overall yield = 96 %; Overall yield = 42 mg; Glovebox; Inert atmosphere;
DOI:10.1002/chem.201303500