2-(1H-1,2,3-benzotriazol-1-ylacetyl)-N-phenylhydrazinecarbothioamide

Base Information

Chemical Name:2-(1H-1,2,3-benzotriazol-1-ylacetyl)-N-phenylhydrazinecarbothioamide
CAS No.:122502-97-0
Molecular Formula:C₁₅H₁₄N₆OS
Molecular Weight:326.382
Hs Code.:
Mol file:122502-97-0.mol

Synonyms:4-phenyl-1-(1-carbonylmethyl-1H-benzotriazole) thiosemicarbazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1H-1,2,3-benzotriazol-1-ylacetyl)-N-phenylhydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-(1H-1,2,3-benzotriazol-1-ylacetyl)-N-phenylhydrazinecarbothioamide

There total 3 articles about 2-(1H-1,2,3-benzotriazol-1-ylacetyl)-N-phenylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 122502-94-7
2-(1H-benzo[d][1,2,3]triazol-1-yl)acetohydrazide

: 103-72-0
phenyl isothiocyanate

: 122502-97-0
4-phenyl-1-(1-carbonylmethyl-1H-benzotriazole) thiosemicarbazide

Guidance literature:: In ethanol; for 0.25h; Heating;
DOI:10.1002/jhet.5570260131

Reference yield:

: 69218-46-8
ethyl (1H-benzotriazol-1-yl)acetate

: 122502-97-0
4-phenyl-1-(1-carbonylmethyl-1H-benzotriazole) thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / hydrazine hydrate / ethanol / 1 h / Heating

2: 75 percent / ethanol / 0.25 h / Heating

With hydrazine hydrate; In ethanol;
DOI:10.1002/jhet.5570260131

Reference yield:

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 122502-97-0
4-phenyl-1-(1-carbonylmethyl-1H-benzotriazole) thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / 1,4-dioxane / 6 h / Reflux

2: hydrazine hydrate / 1,4-dioxane / 5 h / Reflux

3: tetrachloromethane / 2.5 h / Reflux

With potassium carbonate; hydrazine hydrate; In 1,4-dioxane; tetrachloromethane;