2--6-tert-butyl-4-methylphenyl acetate

Base Information

Chemical Name:2--6-tert-butyl-4-methylphenyl acetate
CAS No.:147297-90-3
Molecular Formula:C₂₅H₂₆N₂O₂
Molecular Weight:386.494
Hs Code.:

2-<N-(9H-carbazol-9-yl)amino>-6-tert-butyl-4-methylphenyl acetate

Synonyms:2--6-tert-butyl-4-methylphenyl acetate

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Chemical Property of 2--6-tert-butyl-4-methylphenyl acetate

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Technology Process of 2--6-tert-butyl-4-methylphenyl acetate

There total 3 articles about 2--6-tert-butyl-4-methylphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 2-tert-butyl-6-<(2'-iodo-1,1'-biphenyl-2-yl)azo>-4-methylphenyl acetate

: N-(9H-carbazol-9-yl)-N-(3-tert-butyl-2-hydroxy-5-methylphenyl)acetamide

: 147297-90-3
2--6-tert-butyl-4-methylphenyl acetate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 1h; Heating;
DOI:10.1021/jo00061a013

Reference yield:

: 54147-90-9
2'-iodo-[1,1'-biphenyl]-2-amine

: 147297-90-3
2--6-tert-butyl-4-methylphenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) sodium hydroxide / 1.) diazotation, 0-5 deg C, 2.) water, 0-5 deg C

2: 1.) sodium ethoxide / 1.) ethanol, 2.) benzene, reflux

3: 26 percent / tri-n-butyl hydride, AIBN / benzene / 1 h / Heating; other 2-<(2'-iodo-1,1'-biphenyl-2-yl)azo>-4-methylphenyl acylates

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl hydride; sodium ethanolate; In benzene;
DOI:10.1021/jo00061a013

Reference yield:

: 147297-82-3
2-tert-butyl-6-<(2'-iodo-1,1'-biphenyl-2-yl)azo>-4-methylphenol

: 147297-90-3
2--6-tert-butyl-4-methylphenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium ethoxide / 1.) ethanol, 2.) benzene, reflux

2: 26 percent / tri-n-butyl hydride, AIBN / benzene / 1 h / Heating; other 2-<(2'-iodo-1,1'-biphenyl-2-yl)azo>-4-methylphenyl acylates

With 2,2'-azobis(isobutyronitrile); tri-n-butyl hydride; sodium ethanolate; In benzene;
DOI:10.1021/jo00061a013