allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate

Base Information

Chemical Name:allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate
CAS No.:637741-26-5
Molecular Formula:C₃₉H₆₂O₅
Molecular Weight:610.918
Hs Code.:

Synonyms:allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate

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Chemical Property of allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate

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Technology Process of allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate

There total 2 articles about allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 637742-18-8
(2E,6E,8E)-(4R,5S,10S,11R,12S)-11-(4-Methoxy-benzyloxy)-2,4,6,8,10,12-hexamethyl-5-triethylsilanyloxy-docosa-2,6,8-trienoic acid allyl ester

: 637741-26-5
allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate

Guidance literature:: With hydrogenchloride; In ethanol; at 20 ℃; for 12h;
DOI:10.1039/b305818b

Reference yield:

: 331625-63-9
(2E,6E,8E)-(4R,5S,10S,11R,12S)-11-(4-Methoxy-benzyloxy)-2,4,6,8,10,12-hexamethyl-5-triethylsilanyloxy-docosa-2,6,8-trienoic acid

: 637741-26-5
allyl (2E,4R,5S,6E,8E,10S,11R,12S)-2,4,6,8,10,12-hexamethyl-5-hydroxy-11-(4-methoxybenzyloxy)-2,6,8-docosatrienoate

Guidance literature:: Multi-step reaction with 2 steps

1: cesium hydrogen carbonate / dimethylformamide / 2 h / 20 °C

2: 142 mg / aq. HCl / ethanol / 12 h / 20 °C

With hydrogenchloride; cesium bicarbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/b305818b