tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

Base Information

Chemical Name:tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate
CAS No.:1402612-59-2
Molecular Formula:C₂₄H₃₃N₃O₆S
Molecular Weight:491.609
Hs Code.:

Synonyms:tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

Suppliers and Price of tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

Chemical Property:

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

There total 4 articles about tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: tert-butyl (5-{[(2-nitrophenyl)sulfonyl]amino}pentyl)carbamate

: 103-63-9
1-phenyl-2-bromoethane

: 1402612-59-2
tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

Guidance literature:: With caesium carbonate; In acetonitrile; at 80 ℃; for 18h;
DOI:10.1039/c8ob01499j

Reference yield:

: 51644-96-3
5-tert-butoxycarbonylamino-1-aminopentane

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1402612-59-2
tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: caesium carbonate / acetonitrile / 2 h / 80 °C / Inert atmosphere

With caesium carbonate; triethylamine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 51644-96-3
5-tert-butoxycarbonylamino-1-aminopentane

: 1402612-59-2
tert-butyl (5-((2-nitro-N-phenethylphenyl)sulfonamido)pentyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1.5 h

2: caesium carbonate / acetonitrile / 18 h / 80 °C

With caesium carbonate; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c8ob01499j