5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran

Base Information

• Chemical Name: 5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran
• CAS No.: 131729-46-9
• Molecular Formula: C₂₉H₄₉NO₄
• Molecular Weight: 475.712
• Mol file: 131729-46-9.mol

Synonyms:5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran

Chemical Property of 5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran

There total 3 articles about 5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

pentadecanyl isocyanate (39633-51-7) + 5-<(benzyloxy)methyl>tetrahydrofuran-2-methanol (79494-91-0) → 5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran (131729-46-9)

Guidance literature:

With pyridine; at 70 ℃; for 4h;

DOI:10.1021/jm00105a058

Reference yield:

benzyloxyacetoaldehyde (60656-87-3) → 5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran (131729-46-9)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether / 1 h / Heating

2: 75 percent / m-chloroperbenzoic acid (MCPBA) / CH₂Cl₂ / 24 h / Ambient temperature

3: 76 percent / pyridine / 4 h / 70 °C

With pyridine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;

DOI:10.1021/jm00105a058

Reference yield:

1-O-Benzylhex-5-ene-1,2-diol (131830-52-9) → 5-<<(N-pentadecylcarbamoyl)oxy>methyl>-2-<(benzyloxy)methyl>tetrahydrofuran (131729-46-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / m-chloroperbenzoic acid (MCPBA) / CH₂Cl₂ / 24 h / Ambient temperature

2: 76 percent / pyridine / 4 h / 70 °C

With pyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/jm00105a058

upstream raw materials:

pentadecanyl isocyanate

5-<(benzyloxy)methyl>tetrahydrofuran-2-methanol

benzyloxyacetoaldehyde

1-O-Benzylhex-5-ene-1,2-diol