aminothioacetic acid S-benzyl ester

Base Information

• Chemical Name: aminothioacetic acid S-benzyl ester
• CAS No.: 754172-97-9
• Molecular Formula: C₉H₁₁NOS
• Molecular Weight: 181.258
• Mol file: 754172-97-9.mol

Synonyms:aminothioacetic acid S-benzyl ester

Chemical Property of aminothioacetic acid S-benzyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of aminothioacetic acid S-benzyl ester

There total 1 articles about aminothioacetic acid S-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tert-butoxycarbonylaminothioacetic acid S-benzyl ester (667905-05-7) → aminothioacetic acid S-benzyl ester (754172-97-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

DOI:10.1039/b309196a

Reference yield: 84.0%

aminothioacetic acid S-benzyl ester (754172-97-9) + 7-(diethylamino)coumarin-3-carboxylic acid (50995-74-9) → C23H24N2O4S (1334224-80-4)

Guidance literature:

7-(diethylamino)coumarin-3-carboxylic acid; With triethylamine; HATU; In tetrahydrofuran; for 0.166667h; Cooling with ice;

aminothioacetic acid S-benzyl ester; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1002/anie.201100840

Reference yield: 68.0%

aminothioacetic acid S-benzyl ester (754172-97-9) + 4-carboxybenzophenone (611-95-0) → (4-benzoylbenzoylamino)thioacetic acid S-benzyl ester

Guidance literature:

4-carboxybenzophenone; With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; for 0.5h; cooling;

aminothioacetic acid S-benzyl ester; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 6h; Further stages.;

DOI:10.1039/b309196a

upstream raw materials:

tert-butoxycarbonylaminothioacetic acid S-benzyl ester

Downstream raw materials:

C₂₃H₂₄N₂O₄S