4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone

Base Information

Chemical Name:4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone
CAS No.:1349856-70-7
Molecular Formula:C₂₈H₂₆O₅S₂
Molecular Weight:506.643
Hs Code.:

Synonyms:4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone

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Chemical Property of 4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone

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Technology Process of 4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone

There total 6 articles about 4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 1349856-69-4
C₃₈H₄₂O₇S₂

: 1349856-70-7
4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone

Guidance literature:: With methanol; toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield:

: 71597-85-8
(p-hydroxyphenyl)boronic acid

: 1349856-70-7
4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 10 h / 90 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C

2.2: 5 h / 20 - 60 °C

3.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 20 h / 90 °C

4.1: toluene-4-sulfonic acid; methanol / tetrahydrofuran / 12 h / 20 °C

With methanol; sodium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 80-07-9,30605-10-8,85228-26-8,36313-66-3
4,4'-dichlorodiphenyl sulphone

: 1349856-70-7
4-(4-(2-hydroxyethylthio)phenyl)-4'-(4-(2-hydroxyethyloxy)phenyl)diphenyl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 10 h / 90 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C

2.2: 5 h / 20 - 60 °C

3.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 20 h / 90 °C

4.1: toluene-4-sulfonic acid; methanol / tetrahydrofuran / 12 h / 20 °C

With methanol; sodium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; mineral oil;