Technology Process of C32H38O8
There total 10 articles about C32H38O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: O3 / methanol / -78 °C
2: BH3*THF / tetrahydrofuran / 0 °C
3: PCC / CH2Cl2
4: benzene / Heating
5: 1) Zn / 1) THF, reflux 2) THF, 0 deg C
6: MnO2 / ethyl acetate / Ambient temperature
7: 1) Cs2CO3 2) TFA / 1) CHCl3, r.t. 2) PhH, reflux
8: 77 percent / p-TsOH / benzene / Heating
9: 71 percent / p-TsOH / benzene / Heating
10: 81 percent / m-CPBA / CH2Cl2
With
manganese(IV) oxide; borane-THF; caesium carbonate; toluene-4-sulfonic acid; ozone; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; trifluoroacetic acid; zinc;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; benzene;
DOI:10.1016/S0040-4039(00)94472-1
- Guidance literature:
-
Multi-step reaction with 7 steps
1: benzene / Heating
2: 1) Zn / 1) THF, reflux 2) THF, 0 deg C
3: MnO2 / ethyl acetate / Ambient temperature
4: 1) Cs2CO3 2) TFA / 1) CHCl3, r.t. 2) PhH, reflux
5: 77 percent / p-TsOH / benzene / Heating
6: 71 percent / p-TsOH / benzene / Heating
7: 81 percent / m-CPBA / CH2Cl2
With
manganese(IV) oxide; caesium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; zinc;
In
dichloromethane; ethyl acetate; benzene;
DOI:10.1016/S0040-4039(00)94472-1
