1,1'-bis[5-phenyloxazolin-2-yl]ferrocene

Base Information

• Chemical Name: 1,1'-bis[5-phenyloxazolin-2-yl]ferrocene
• CAS No.: 877175-67-2
• Molecular Formula: C₂₈H₂₄FeN₂O₂
• Molecular Weight: 476.358
• Mol file: 877175-67-2.mol

Synonyms:1,1'-bis[5-phenyloxazolin-2-yl]ferrocene

Chemical Property of 1,1'-bis[5-phenyloxazolin-2-yl]ferrocene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1'-bis[5-phenyloxazolin-2-yl]ferrocene

There total 1 articles about 1,1'-bis[5-phenyloxazolin-2-yl]ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

[C5H4CONHCH2CH(C6H5)OH]2Fe (877175-53-6) → 1,1'-bis[5-phenyloxazolin-2-yl]ferrocene (877175-67-2)

Guidance literature:

With p-toluenesulfonyl chloride; triethylamine; catalyst: 4-(dimethylamino)pyridine; In dichloromethane; (Ar), soln. of p-toluenesulfonyl chloride in CH2Cl2 added dropwise at 0°C to soln. of Fe complex, Et3N and catalyst: 4-(dimethylamino)pyridine in CH2Cl2, stirred at room temp. for 10 h; washed *sat. soln. of NaHCO3, brine), water layer extd.(CH2Cl2), org. phase dried (Na2SO4), chromy.(silica gel - ethyl acetate/n-hexane), elem. anal.;

DOI:10.1002/ejic.200400737

upstream raw materials:

[C₅H₄CONHCH₂CH(C₆H₅)OH]2Fe