C₃₅H₃₆F₂O₆

Base Information

Chemical Name:C₃₅H₃₆F₂O₆
CAS No.:1413374-91-0
Molecular Formula:C₃₅H₃₆F₂O₆
Molecular Weight:590.664
Hs Code.:

C<sub>35</sub>H<sub>36</sub>F<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₅H₃₆F₂O₆

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Chemical Property of C₃₅H₃₆F₂O₆

Chemical Property:

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Technology Process of C₃₅H₃₆F₂O₆

There total 21 articles about C₃₅H₃₆F₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1S,3R,4R,5S,6S)-4,5,6-tris(benzyloxy)-3-[(benzyl)methyl]-2,2-difluorocyclohexanol

: 1027745-76-1
(3R,4R,5S,6S)-4,5,6-tris(benzyloxy)-3-[(benzyl)methyl]-2,2-difluorocyclohexanone

: 1413374-91-0
C₃₅H₃₆F₂O₆

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1027745-76-1
(3R,4R,5S,6S)-4,5,6-tris(benzyloxy)-3-[(benzyl)methyl]-2,2-difluorocyclohexanone

: 1413374-91-0
C₃₅H₃₆F₂O₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

5.2: 0.75 h

6.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 12 h / 40 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 2 h / 0 - 20 °C

8.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

9.1: hydrogenchloride; methanol / dichloromethane / 20 °C

10.1: pyridine / dmap / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

11.1: diethylamino-sulfur trifluoride / dichloromethane / 16 h / 20 °C / Inert atmosphere

12.1: sodium methylate; methanol / 20 °C / Industry scale

13.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; methanol; oxalyl dichloride; diethylamino-sulfur trifluoride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; sodium methylate; Dess-Martin periodane; dimethyl sulfoxide; L-proline; trichlorophosphate; dmap; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1027745-76-1
(3R,4R,5S,6S)-4,5,6-tris(benzyloxy)-3-[(benzyl)methyl]-2,2-difluorocyclohexanone

: 1413374-91-0
C₃₅H₃₆F₂O₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

5.2: 0.75 h

6.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 12 h / 40 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 2 h / 0 - 20 °C

8.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

9.1: hydrogenchloride; methanol / dichloromethane / 20 °C

10.1: pyridine / dmap / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

11.1: diethylamino-sulfur trifluoride / dichloromethane / 16 h / 20 °C / Inert atmosphere

12.1: sodium methylate; methanol / 20 °C / Industry scale

13.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; methanol; sodium tetrahydroborate; n-butyllithium; diethylamino-sulfur trifluoride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; sodium methylate; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; trifluoroacetic anhydride; dmap; 18-crown-6 ether; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;