N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide

Base Information

• Chemical Name: N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide
• CAS No.: 597540-88-0
• Molecular Formula: C₂₁H₃₁NO₂S
• Molecular Weight: 361.549

Synonyms:N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide

Chemical Property of N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide

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Technology Process of N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide

There total 1 articles about N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

prenyl bromide (870-63-3) + (4S)-5-methyl-4-[N-(2,4,6-trimethylbenzenesulfonyl)amino]-1,2-hexadiene (220765-22-0) → N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide (597540-88-0)

Guidance literature:

(4S)-5-methyl-4-[N-(2,4,6-trimethylbenzenesulfonyl)amino]-1,2-hexadiene; With sodium hydride; In N,N-dimethyl-formamide;

prenyl bromide; In N,N-dimethyl-formamide;

DOI:10.1002/chem.200500050

Reference yield: 82.0%

N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide (597540-88-0) → (1R,4S)-3-aza-4-isopropyl-8,8-dimethyl-3-(2,4,6-trimethylphenylsulfonyl)bicyclo[4.2.0]oct-5-ene

Guidance literature:

In N,N-dimethyl-formamide; for 24h; Heating;

DOI:10.1002/anie.200501413 DOI:10.1021/jo0700528

Reference yield: 45.0%

N-[(1S)-1-(2-isopropyl)buta-2,3-dienyl]-2,4,6-trimethyl-N-(3-methyl-2-butenyl)phenylsulfonamide (597540-88-0) + para-iodoanisole (696-62-8) → (3S,4S,7S)-5-aza-4-isopropyl-11-methoxy-8,8-dimethyl-2-methylene-5-(2,4,6-trimethylphenylsulfonyl)tricyclo[7.4.0.03,7]trideca-1(9),10,12-triene

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 30h; Heating;

DOI:10.1002/chem.200500050

upstream raw materials:

prenyl bromide

(4S)-5-methyl-4-[N-(2,4,6-trimethylbenzenesulfonyl)amino]-1,2-hexadiene

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