5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine

Base Information

Chemical Name:5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine
CAS No.:1037627-97-6
Molecular Formula:C₄₃H₂₆F₁₅IrN₆
Molecular Weight:1103.92
Hs Code.:

Synonyms:5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine

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Chemical Property of 5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine

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Technology Process of 5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine

There total 3 articles about 5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 5,10,15-tris(pentafluorophenyl)corrole

: 1037627-97-6
5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine

Guidance literature:: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 5,10,15-tris(pentafluorophenyl)corrole; With trimethylamine-N-oxide; potassium carbonate; In tetrahydrofuran; for 1.5h; Inert atmosphere; Reflux;

In tetrahydrofuran; at 20 ℃; Inert atmosphere; Reflux;

Reference yield: 27.0%

: 1184-78-7
trimethylamine-N-oxide

: 5,10,15-tris(pentafluorophenyl)corrole

: 1037627-97-6
5,10,15-tris(pentafluorophenyl)corrolatoiridium(III) bis(trimethylamine)

Guidance literature:: 5,10,15-tris(pentafluorophenyl)corrole; With bis(1,5-cyclooctadiene)diiridium(I) dichloride; potassium carbonate; In tetrahydrofuran; Reflux; Inert atmosphere;

trimethylamine-N-oxide; In tetrahydrofuran; at 20 ℃; Heating;
DOI:10.1021/ja801049t

Reference yield: 27.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 1184-78-7
trimethylamine-N-oxide

: 5,10,15-tris(pentafluorophenyl)corrole

: 1037627-97-6
5,10,15-tris-pentafluorophenylcorrolato-iridium(III) bis-trimethylamine

Guidance literature:: With potassium carbonate; In tetrahydrofuran; under Ar atm. Ir complex, corrole and K2CO3 in THF were refluxed for 90 min, tma N-oxide was added and allowed to cool to room temp. in air; column chromy. on silica (hexane - CH2Cl2 4:1);
DOI:10.1021/ja801049t