(E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

Base Information

Chemical Name:(E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene
CAS No.:732298-08-7
Molecular Formula:C₄₃H₃₈O₅
Molecular Weight:634.772
Hs Code.:

Synonyms:(E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

Suppliers and Price of (E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

There total 7 articles about (E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 120980-04-3
(E)-1-(2,4-bis(benzyloxy)-6-hydroxyphenyl)-3-(3',4'-bis(benzyloxy)phenyl)prop-2-en-1-one

: 732298-08-7
(E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

Guidance literature:: (E)-1-(2,4-bis(benzyloxy)-6-hydroxyphenyl)-3-(3',4'-bis(benzyloxy)phenyl)prop-2-en-1-one; With water; In tetrahydrofuran; ethanol; at -1.5 - 20 ℃;

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at -0.8 - -0.3 ℃;
DOI:10.3390/molecules15085595

Reference yield: 60.0%

: 63604-98-8
1,3-dibenzylphloroglucinol

: 362632-29-9
(E)-3-(3,4-bis(benzyloxy)phenyl)prop-2-en-1-ol

: 732298-08-7
(E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

Guidance literature:: With montmorillonite K-10; In dichloromethane; at 20 ℃; for 15.5h; Inert atmosphere;
DOI:10.1039/c7ob02837g

Reference yield:

: 5447-02-9
3,4-dibenzyloxybenzaldehyde

: 732298-08-7
(E)-3-[2,4-bis(benzyloxy)-6-hydroxyphenyl]-1-[3,4-bis(benzyloxy)phenyl]propene

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran; various solvent(s) / 2 h / 20 °C

2: 7.9 g / DIBAL / tetrahydrofuran; hexane / 2 h / -78 - 20 °C

3: 47.3 percent / silica gel supported H₂SO₄ / CH₂Cl₂ / 20 °C

With sulfuric acid; silica gel; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane; 3: Friedel-Craft alkylation;
DOI:10.1016/j.bmc.2004.04.033