cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate

Base Information

Chemical Name:cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate
CAS No.:632620-13-4
Molecular Formula:C₁₅H₂₄O₆
Molecular Weight:300.352
Hs Code.:

Synonyms:cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate

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Chemical Property of cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate

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Technology Process of cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate

There total 4 articles about cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6998-83-0
trimethyl cis,cis-cyclohexane-1,3,5-tricarboxylate

: 108-24-7
acetic anhydride

: 632620-13-4
cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate

Guidance literature:: trimethyl cis,cis-cyclohexane-1,3,5-tricarboxylate; With lithium aluminium tetrahydride; In tetrahydrofuran; for 73h; Heating / reflux;

With acetic acid; In tetrahydrofuran;

acetic anhydride; at 90 - 140 ℃; for 5h;

Reference yield: 83.0%

: 5962-82-3,72890-46-1
cis,cis-1,3,5-tris(hydroxymethyl)cyclohexane

: 108-24-7
acetic anhydride

: 632620-13-4
cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate

Guidance literature:: at 100 ℃; for 1h;
DOI:10.1021/ja0361291

Reference yield:

: 69464-55-7
3-methoxy-7-(methoxymethyl)-3-borabicyclo[3,3,1]non-6-ene

: 632620-13-4
cis-1,3,5-tris(hydroxymethyl)cyclohexane triacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / 1 h / Heating

2: 76 percent / trimethylamine N-oxide dihydrate / toluene / 16 h / Heating

3: 83 percent / 1 h / 100 °C

With trimethylamine-N-oxide; In toluene;
DOI:10.1021/ja0361291