4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester

Base Information

Chemical Name:4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester
CAS No.:77442-00-3
Molecular Formula:C₁₆H₁₅N₇O₄S
Molecular Weight:401.406
Hs Code.:

Synonyms:4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester

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Chemical Property of 4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester

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Technology Process of 4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester

There total 4 articles about 4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77441-93-1
C₁₀H₁₂N₄O₂S

: 77442-00-3
4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 87.8 percent / Na₂CO₃ / H₂O / 3 h / Heating

2: 1) 37 percent HCl, NaNO₂; 2) CH₃COONa / 1) H₂O, 0-5 degC, 15 min.; 2) H₂O, 0-5 degC, 24 h

With hydrogenchloride; sodium acetate; sodium carbonate; sodium nitrite; In water;

Reference yield:

: 6296-41-9
p-Aminophenylbrenztraubensaeurehydrochlorid

: 77442-00-3
4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 93.4 percent / CH₃COONa / H₂O / Heating

2: 87.8 percent / Na₂CO₃ / H₂O / 3 h / Heating

3: 1) 37 percent HCl, NaNO₂; 2) CH₃COONa / 1) H₂O, 0-5 degC, 15 min.; 2) H₂O, 0-5 degC, 24 h

With hydrogenchloride; sodium acetate; sodium carbonate; sodium nitrite; In water;

Reference yield:

: 18692-67-6
2-Phenyl-4-(p-acetylaminobenzyliden)-5-oxazolon

: 77442-00-3
4-(2-Thio-6-azauracil-5-yl-methyl)phenylhydrazonocyanacetylcarbamidsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KOH / 1) H₂O, 6 h, reflux; 2) 1.5 h, reflux

2: 1) 37 percent HCl, NaNO₂; 2) CH₃COONa / 1) H₂O, 0-5 degC, 15 min.; 2) H₂O, 0-5 degC, 24 h

With hydrogenchloride; potassium hydroxide; sodium acetate; sodium nitrite;