C₁₄H₁₈O₄

Base Information

Chemical Name:C₁₄H₁₈O₄
CAS No.:1622095-24-2
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:

C<sub>14</sub>H<sub>18</sub>O<sub>4</sub>

Synonyms:C₁₄H₁₈O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₈O₄

Chemical Property:

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Technology Process of C₁₄H₁₈O₄

There total 7 articles about C₁₄H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1622095-22-0
C₁₅H₁₈O₅

: 1622095-24-2
C₁₄H₁₈O₄

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; cyclohexane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201402096

Reference yield:

: 99865-70-0
4-(4-Formyl-phenoxy)butyric acid

: 1622095-24-2
C₁₄H₁₈O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 14 h / 20 °C

2.1: dichloromethane / 14 h / 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

3.2: 11.5 h / -78 - -5 °C

4.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 1.5 h / Cooling with ice

5.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

With dmap; lithium hydroxide monohydrate; dihydrogen peroxide; sodium hexamethyldisilazane; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; cyclohexane; water; 2.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096

Reference yield:

: 1622095-18-4
C₂₄H₂₅NO₆

: 1622095-24-2
C₁₄H₁₈O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

1.2: 11.5 h / -78 - -5 °C

2.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 1.5 h / Cooling with ice

3.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

With lithium hydroxide monohydrate; dihydrogen peroxide; sodium hexamethyldisilazane; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; cyclohexane; water;
DOI:10.1002/ejoc.201402096