2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester

Base Information

Chemical Name:2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester
CAS No.:816426-19-4
Molecular Formula:C₅₃H₄₇O₁₁PS₂
Molecular Weight:955.055
Hs Code.:

Synonyms:2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester

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Chemical Property of 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester

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Technology Process of 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester

There total 1 articles about 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1005-56-7
phenylcarbonochloridothioate

: 376590-85-1
1-O-diphenylphosphate-2,4,6-tri-O-benzyl-D-myo-inositol

: 816426-19-4
2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester

Guidance literature:: With pyridine; dmap; In dichloromethane; for 24h;
DOI:10.1021/ja047360x

Reference yield: 60.0%

: 816426-19-4
2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester

: 816426-20-7
2,4,6-tri-O-benzyl-D-myo-inositol-3,5-dideoxy-1-diphenyl phosphate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Heating;
DOI:10.1021/ja047360x

Reference yield:

: 816426-19-4
2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3,5-O-dithiocarbonic acid diphenylester

: Phosphoric acid benzyl ester (2R,6R)-2,4,6-tris-benzyloxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / Bu₃SnH; AIBN / toluene

2: 67 percent / NaH / tetrahydrofuran / 3 h

3: LiBr / acetone / 12 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; lithium bromide; In tetrahydrofuran; acetone; toluene;
DOI:10.1021/jo060702s