{N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone

Base Information

Chemical Name:{N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone
CAS No.:1313739-72-8
Molecular Formula:C₂₀H₂₁IN₂O₃S
Molecular Weight:496.369
Hs Code.:

Synonyms:{N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone

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Chemical Property of {N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone

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Technology Process of {N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone

There total 3 articles about {N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313739-71-7
2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl p-toluenesulfonate

: 1313739-72-8
{N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / ethanol; acetonitrile / 24 h / 85 °C / sealed tube

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 5 h / Reflux

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In ethanol; acetonitrile;
DOI:10.1039/c1ob05087g

Reference yield:

: 455254-73-6
N-phenylsulfonyl-2-iodotryptophol

: 1313739-72-8
{N-[2-(2-iodo-1-phenylsulfonyl-1H-indol-3-yl)ethyl]-N-methylamino}-2-propanone

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2: potassium carbonate / ethanol; acetonitrile / 24 h / 85 °C / sealed tube

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 5 h / Reflux

With dmap; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; acetonitrile;
DOI:10.1039/c1ob05087g