2-imino-3-phenyl-4-thiazolidinone

Base Information

• Chemical Name: 2-imino-3-phenyl-4-thiazolidinone
• CAS No.: 131842-14-3
• Molecular Formula: C₁₈H₁₄N₄O₂S₃
• Molecular Weight: 414.533

Synonyms:2-imino-3-phenyl-4-thiazolidinone

Chemical Property of 2-imino-3-phenyl-4-thiazolidinone

Chemical Property:

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Technology Process of 2-imino-3-phenyl-4-thiazolidinone

There total 5 articles about 2-imino-3-phenyl-4-thiazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

N1-(benzothiazole-2-ylthioacetyl)-N4-phenyl-3-thiosemicarbazide (116710-42-0) + chloroacetic acid (79-11-8) → 2-imino-3-phenyl-4-thiazolidinone (131842-14-3)

Guidance literature:

With sodium acetate; In ethanol; for 8h; Heating;

DOI:10.1023/A:1023772509165

Reference yield:

[(1,3-benzothiazol-2-ylthio)acetyl]hydrazine (24044-91-5) → 2-imino-3-phenyl-4-thiazolidinone (131842-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / propan-2-ol / Heating

2: 68 percent / AcONa / ethanol / 8 h / Heating

With sodium acetate; In ethanol; isopropyl alcohol;

DOI:10.1023/A:1023772509165

Reference yield:

phenyl isothiocyanate (103-72-0) → 2-imino-3-phenyl-4-thiazolidinone (131842-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / propan-2-ol / Heating

2: 68 percent / AcONa / ethanol / 8 h / Heating

With sodium acetate; In ethanol; isopropyl alcohol;

DOI:10.1023/A:1023772509165

upstream raw materials:

N¹-(benzothiazole-2-ylthioacetyl)-N⁴-phenyl-3-thiosemicarbazide

chloroacetic acid

phenyl isothiocyanate

[(1,3-benzothiazol-2-ylthio)acetyl]hydrazine

Downstream raw materials:

(Benzothiazol-2-ylsulfanyl)-acetic acid [5-[1-(4-chloro-phenyl)-meth-(Z)-ylidene]-4-oxo-3-phenyl-thiazolidin-(2E)-ylidene]-hydrazide

2-imino-5-benzylidene-3-phenyl-4-thiazolidinone

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