C₃₂H₃₀N₂O₅

Base Information

• Chemical Name: C₃₂H₃₀N₂O₅
• CAS No.: 1402135-50-5
• Molecular Formula: C₃₂H₃₀N₂O₅
• Molecular Weight: 522.601
• Mol file: 1402135-50-5.mol

Synonyms:C₃₂H₃₀N₂O₅

Chemical Property of C₃₂H₃₀N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₃₀N₂O₅

There total 11 articles about C₃₂H₃₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.58%

C39H36N2O5 (1402135-42-5) → C32H30N2O5 (1402135-50-5)

Guidance literature:

With palladium 10% on activated carbon; In methanol; for 12h; under 30003 Torr;

DOI:10.1021/jm300985d

Reference yield:

tert-butyl benzyl(2-(benzyloxy)-2-phenylethyl)carbamate (1402135-35-6) → C32H30N2O5 (1402135-50-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane

2.1: triethylamine / tetrahydrofuran / 0 °C

2.2: 0 - 20 °C

3.1: palladium 10% on activated carbon / methanol / 12 h / 30003 Torr

With palladium 10% on activated carbon; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1021/jm300985d

Reference yield:

2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)-carbamoyl)benzoic acid (1402135-34-5) → C32H30N2O5 (1402135-50-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: lithium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

2.1: oxalyl dichloride / tetrahydrofuran / 0.5 h / 0 °C

3.1: triethylamine / tetrahydrofuran / 0 °C

3.2: 0 - 20 °C

4.1: palladium 10% on activated carbon / methanol / 12 h / 30003 Torr

With oxalyl dichloride; palladium 10% on activated carbon; water; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol;

DOI:10.1021/jm300985d

upstream raw materials:

tert-butyl benzyl(2-(benzyloxy)-2-phenylethyl)carbamate

2-((1-chloro-1-oxo-3-phenylpropan-2-yl)carbamoyl)benzoic acid

phthalic anhydride

C₃₉H₃₆N₂O₅