3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester

Base Information

• Chemical Name: 3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester
• CAS No.: 185844-42-2
• Molecular Formula: C₁₇H₂₆O₂SSi
• Molecular Weight: 322.544

Synonyms:3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester

Chemical Property of 3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester

Chemical Property:

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Technology Process of 3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester

There total 1 articles about 3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(Dimethyl-phenyl-silanyl)-butan-1-one (120627-94-3) → 3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester (185844-42-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / HCl, H₂S / diethyl ether / -30 °C

2: 80 percent / K₂CO₃ / acetone / Ambient temperature

With hydrogenchloride; hydrogen sulfide; potassium carbonate; In diethyl ether; acetone;

DOI:10.1039/P19960002803

Reference yield: 48.0%

3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester (185844-42-2) → 3-(1-Phenyl-butylsulfanyl)-propionic acid ethyl ester

Guidance literature:

With cesium fluoride; In acetonitrile; at 82 ℃;

DOI:10.1039/P19960002803

Reference yield: 30.0%

3-[(Z)-1-(Dimethyl-phenyl-silanyl)-but-1-enylsulfanyl]-propionic acid ethyl ester (185844-42-2) + 3-[(Z)-1-(Dimethyl-phenyl-silanyl)-3-methyl-but-1-enylsulfanyl]-propionic acid methyl ester (199847-75-1) → 3-(1-Phenyl-butylsulfanyl)-propionic acid ethyl ester + 3-(1-Phenyl-butylsulfanyl)-propionic acid methyl ester + 3-(3-Methyl-1-phenyl-butylsulfanyl)-propionic acid methyl ester + 3-(3-Methyl-1-phenyl-butylsulfanyl)-propionic acid ethyl ester

Guidance literature:

With aq. TBFF; In tetrahydrofuran; for 5h; Heating;

upstream raw materials:

1-(Dimethyl-phenyl-silanyl)-butan-1-one

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