(1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

Base Information

Chemical Name:(1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol
CAS No.:1252047-56-5
Molecular Formula:C₃₁H₅₂N₂O₈Si
Molecular Weight:608.848
Hs Code.:

(1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

Synonyms:(1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

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Chemical Property of (1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

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Technology Process of (1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

There total 2 articles about (1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1252047-50-9
C₃₁H₅₀N₂O₈Si

: 1252047-56-5
(1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

: 1252047-58-7
(1S)-1-[(2R,3R,5S,6S)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 16h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tet.2010.07.037

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 1252047-49-6
C₂₂H₃₂N₂O₈

: 1252047-56-5
(1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

Guidance literature:: With pyridine; at 50 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2010.07.037

Reference yield: 100.0%

: 1252047-56-5
(1R)-1-[(2R,3R,5R,6R)-3-[(R)-1H-imidazol-2-yl-[(4-methoxyphenyl)methoxy]methyl]-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-2-triisopropylsilyloxy-ethanol

: 1252047-57-6
(2S,3S,4aS,5R,10S,10aR)-2,3-dimethoxy-5-((4-methoxybenzyl)oxy)-2,3-dimethyl-10-(((triisopropylsilyl)oxy)methyl)-2,3,4a,5,10,10a-hexahydro-[1,4]dioxino[2,3-d]imidazo[1,2-a]pyridine

Guidance literature:: With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -15 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.07.037