cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane

Base Information

Chemical Name:cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane
CAS No.:196516-14-0
Molecular Formula:C₂₃H₃₃N₃O₄S₂
Molecular Weight:479.665
Hs Code.:

Synonyms:cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane

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Chemical Property of cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane

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Technology Process of cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane

There total 1 articles about cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98-59-9
p-toluenesulfonyl chloride

: 173437-79-1
cis-cis-2,4,6-trimethyl-1,3,5-triaminocyclohexane

: 196516-14-0
cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane

Guidance literature:: With triethylamine; In tetrahydrofuran; for 4h; Heating;
DOI:10.1039/a701364g

Reference yield: 90.0%

: 623-24-5
1,4-bis(bromomethyl)benzene

: 196516-14-0
cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane

: 196516-06-0
C₅₄H₇₂N₆O₈S₄

Guidance literature:: With potassium carbonate; In acetonitrile; for 12h; Heating;
DOI:10.1039/a701364g

Reference yield:

: 196516-14-0
cis,cis-1,3-bis(p-tolylsulfonylamino)-5-amino-2,4,6-trimethylcyclohexane

: C₂₆H₄₈N₆

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / potassium carbonate / acetonitrile / 12 h / Heating

2: 72 percent / ammonia; sodium / tetrahydrofuran; ethanol / 2 h / -78 °C

With ammonia; sodium; potassium carbonate; In tetrahydrofuran; ethanol; acetonitrile; 1: Alkylation / 2: detosylation;
DOI:10.1039/a701364g