2-[(4,6,7-Trimethoxy-2,3-dihydro-1-benzofuran-5-yl)methylidene]hydrazine-1-carboximidic acid

Base Information

Chemical Name:2-[(4,6,7-Trimethoxy-2,3-dihydro-1-benzofuran-5-yl)methylidene]hydrazine-1-carboximidic acid
CAS No.:6960-60-7
Molecular Formula:C₁₃H₁₇N₃O₅
Molecular Weight:295.295
Hs Code.:
DSSTox Substance ID:DTXSID70989691
ChEMBL ID:CHEMBL2143640

Synonyms:MLS002667635;CHEMBL2143640;DTXSID70989691;HMS3080M14;SMR001557395;2-[(4,6,7-Trimethoxy-2,3-dihydro-1-benzofuran-5-yl)methylidene]hydrazine-1-carboximidic acid

Suppliers and Price of 2-[(4,6,7-Trimethoxy-2,3-dihydro-1-benzofuran-5-yl)methylidene]hydrazine-1-carboximidic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-[(4,6,7-Trimethoxy-2,3-dihydro-1-benzofuran-5-yl)methylidene]hydrazine-1-carboximidic acid

Chemical Property:

Density:1.39g/cm³
XLogP3:0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:295.11682065
Heavy Atom Count:21
Complexity:392

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C2=C1CCO2)OC)OC)C=NNC(=O)N

Technology Process of 2-[(4,6,7-Trimethoxy-2,3-dihydro-1-benzofuran-5-yl)methylidene]hydrazine-1-carboximidic acid

There total 4 articles about 2-[(4,6,7-Trimethoxy-2,3-dihydro-1-benzofuran-5-yl)methylidene]hydrazine-1-carboximidic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91143-86-1
4,6,7-Trimethoxy-cumaran-3-on

: 6960-60-7
4,6,7-trimethoxy-2,3-dihydro-benzofuran-5-carbaldehyde semicarbazone

Guidance literature:: Multi-step reaction with 4 steps

1: lithium alanate; tetrahydrofuran

2: palladium/charcoal; ethanol / Hydrogenation

3: phosphoryl chloride

With tetrahydrofuran; palladium on activated charcoal; lithium aluminium tetrahydride; ethanol; trichlorophosphate;
DOI:10.1021/jo01094a046

Reference yield:

: 99865-69-7
4,6,7-trimethoxy-benzofuran

: 6960-60-7
4,6,7-trimethoxy-2,3-dihydro-benzofuran-5-carbaldehyde semicarbazone

Guidance literature:: Multi-step reaction with 3 steps

1: palladium/charcoal; ethanol / Hydrogenation

2: phosphoryl chloride

With palladium on activated charcoal; ethanol; trichlorophosphate;
DOI:10.1021/jo01094a046