(S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

Base Information

Chemical Name:(S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester
CAS No.:169940-41-4
Molecular Formula:C₂₄H₃₂O₄Si
Molecular Weight:412.601
Hs Code.:

Synonyms:(S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

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Chemical Property of (S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

Chemical Property:

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Technology Process of (S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

There total 1 articles about (S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51479-73-3
allyl trichloroacetimidate

: 124655-05-6
(S)-methyl 4-(tert-butyldiphenylsilyloxy)-3-hydroxybutanoate

: 169940-41-4
(S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

Guidance literature:: With trifluorormethanesulfonic acid; In cyclohexane; for 70h; Ambient temperature;
DOI:10.1021/jm950588y

Reference yield:

: 169940-41-4
(S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

: 169940-43-6
(S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butan-1-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -75 ℃; for 1.5h; Yield given;
DOI:10.1021/jm950588y

Reference yield:

: 169940-41-4
(S)-3-Allyloxy-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

: 169940-44-7
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-3-(2-hydroxy-ethoxy)-butan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: DIBAL-H / tetrahydrofuran; toluene / 1.5 h / -75 °C

2: 1.) ozone, 2.) NaBH₄ / 1.) MeOH, -78 deg C, 2.) MeOH, from -78 deg C to RT

With sodium tetrahydroborate; diisobutylaluminium hydride; ozone; In tetrahydrofuran; toluene;
DOI:10.1021/jm950588y