(S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate

Base Information

Chemical Name:(S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate
CAS No.:869854-55-7
Molecular Formula:C₂₅H₂₅F₃N₂O₃S
Molecular Weight:490.546
Hs Code.:

Synonyms:(S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate

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Chemical Property of (S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate

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Technology Process of (S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate

There total 6 articles about (S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₁₇F₃N₂O₆S

: 10420-89-0
(S)-1-(1-Naphthyl)ethylamine

: 869854-55-7
(S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate

Guidance literature:: In acetonitrile; at 10 - 30 ℃; for 17.25h;

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 869854-55-7
(S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate

: C₂₅H₂₅F₃N₂O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / N,N-dimethyl-formamide / 1 h / Inert atmosphere

2: neat (no solvent) / 192 - 218 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.58 h / -5 - 15 °C / Inert atmosphere

4: dmap / acetonitrile / 3 h / 20 °C / Inert atmosphere

5: acetonitrile / 17 h / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; dmap; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ml500331y

Reference yield:

: 10345-50-3
O-(4-acetylphenyl) N,N-dimethylcarbamothioate

: 869854-55-7
(S)-2-(4-(dimethylcarbamoylthio)phenyl)-1,1,1-trifluoropropan-2-yl (S)-1-(naphthalen-1-yl)ethylcarbamate

: C₂₅H₂₅F₃N₂O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: neat (no solvent) / 192 - 218 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.58 h / -5 - 15 °C / Inert atmosphere

3: dmap / acetonitrile / 3 h / 20 °C / Inert atmosphere

4: acetonitrile / 17 h / Inert atmosphere

With dmap; tetrabutyl ammonium fluoride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ml500331y