bis(1-methyl-2-(p-tolylazo)imidazole)(p-MeC₆H₄C(NO)NNPh)Ru(II)](ClO₄)

Base Information

• Chemical Name: bis(1-methyl-2-(p-tolylazo)imidazole)(p-MeC₆H₄C(NO)NNPh)Ru(II)](ClO₄)
• CAS No.: 478495-26-0
• Molecular Formula: C₃₆H₃₆N₁₁ORu*ClO₄
• Molecular Weight: 839.276

Synonyms:bis(1-methyl-2-(p-tolylazo)imidazole)(p-MeC₆H₄C(NO)NNPh)Ru(II)](ClO₄)

Chemical Property of bis(1-methyl-2-(p-tolylazo)imidazole)(p-MeC₆H₄C(NO)NNPh)Ru(II)](ClO₄)

Chemical Property:

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Technology Process of bis(1-methyl-2-(p-tolylazo)imidazole)(p-MeC₆H₄C(NO)NNPh)Ru(II)](ClO₄)

There total 1 articles about bis(1-methyl-2-(p-tolylazo)imidazole)(p-MeC₆H₄C(NO)NNPh)Ru(II)](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

cis,trans,cis-diaquobis[1-methyl-2-(p-tolylazo)imidazole]ruthenium(II) diperchlorate + phenylazo-p-tolylaldoxime (24621-45-2) → bis(1-methyl-2-(p-tolylazo)imidazole)(p-MeC6H4C(NO)NNPh)Ru(II)](ClO4) (478495-26-0)

Guidance literature:

With NaOMe; NaClO₄; In methanol; 1 equiv. of N-compd. and NaOMe were added to MeOH soln. of Ru-complex, reflux for 4 h, soln. was cooled and filtered, satd. aq. soln. of NaClO4 was added; ppt. was filtered off, dried, taking in CH2Cl2, chromy. through silica in toluene, elution with toluene:MeCN=3:1, v/v, evapn. on steam bath, drying in vac. over P4O10, elem. anal.;

DOI:10.1039/b204442k

upstream raw materials:

phenylazo-p-tolylaldoxime

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