1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

Base Information

• Chemical Name: 1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol
• CAS No.: 109075-02-7
• Molecular Formula: C₂₅H₃₆N₂O₆S₂
• Molecular Weight: 524.703

Synonyms:1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

Chemical Property of 1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

Chemical Property:

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Technology Process of 1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

There total 6 articles about 1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(S)-2-((4R,5R)-2,2-dimethyl-5-((S)-1-tosylaziridin-2-yl)-1,3-dioxolan-4-yl)-1-tosyl-aziridine (109075-06-1) → 1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol (109075-02-7)

Guidance literature:

In tetrahydrofuran; at -78 - -30 ℃; for 4h;

DOI:10.1021/jo00283a028

Reference yield: 85.0%

(S)-2-((4R,5R)-2,2-dimethyl-5-((S)-1-tosylaziridin-2-yl)-1,3-dioxolan-4-yl)-1-tosyl-aziridine (109075-06-1) → 1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol (109075-02-7)

Guidance literature:

With tetrahydrofuran; at -78 - -30 ℃;

DOI:10.1016/S0040-4039(00)84935-7

Reference yield: 85.0%

(S)-2-((4R,5R)-2,2-dimethyl-5-((S)-1-tosylaziridin-2-yl)-1,3-dioxolan-4-yl)-1-tosyl-aziridine (109075-06-1) → 1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol (109075-02-7)

Guidance literature:

In tetrahydrofuran; 1.) -78 deg C up to -30 deg C within 2h, 2.) -30 deg C 2h;

DOI:10.1016/S0040-4039(00)95507-2

upstream raw materials:

(S)-2-((4R,5R)-2,2-dimethyl-5-((S)-1-tosylaziridin-2-yl)-1,3-dioxolan-4-yl)-1-tosyl-aziridine

1,6-di-O-(p-toluenesulfonyl)-3,4-O-isopropylidene-D-mannitol

1,6-diazido-1,6-dideoxy-3,4-O-methylethylidene-D-mannitol

(2S, 3R, 4R, 5S)-1,2:5,6 diimino 3,4-O-methylethylidene hexane diol

Downstream raw materials:

methyl 2(S)-butanoate

1,2,5,6-tetradeoxy-1,6-dimethyl-2,5-bis-L-iditol

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