(2S,3S,4R)-tert-butyl 2-(benzhydrylamino)-4-[(tert-butyldimethylsilyl)oxy]-3-hydroxypentanoate

Base Information

Chemical Name:(2S,3S,4R)-tert-butyl 2-(benzhydrylamino)-4-[(tert-butyldimethylsilyl)oxy]-3-hydroxypentanoate
CAS No.:1552271-52-9
Molecular Formula:C₂₈H₄₃NO₄Si
Molecular Weight:485.739
Hs Code.:

Synonyms:(2S,3S,4R)-tert-butyl 2-(benzhydrylamino)-4-[(tert-butyldimethylsilyl)oxy]-3-hydroxypentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-tert-butyl 2-(benzhydrylamino)-4-[(tert-butyldimethylsilyl)oxy]-3-hydroxypentanoate

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Technology Process of (2S,3S,4R)-tert-butyl 2-(benzhydrylamino)-4-[(tert-butyldimethylsilyl)oxy]-3-hydroxypentanoate

There total 1 articles about (2S,3S,4R)-tert-butyl 2-(benzhydrylamino)-4-[(tert-butyldimethylsilyl)oxy]-3-hydroxypentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 74262-56-9,87727-28-4,104501-60-2,111819-71-7
(2R)-2-(tert-butyldimethylsilyloxy)propanal

: 1552271-52-9
(2S,3S,4R)-tert-butyl 2-(benzhydrylamino)-4-[(tert-butyldimethylsilyl)oxy]-3-hydroxypentanoate

Guidance literature:: N-(diphenylmethylene)glycine tert-butyl ester; (2R)-2-(tert-butyldimethylsilyloxy)propanal; With ((2S,2'S,5S,5’S)-1,1'-((2-hydroxy-5-methyl-1,3-phenylene)-bis-(methylene))-bis-(5-phenylpyrrolidine-2,1-diyl))-bis-(diphenylmethanol); diethylzinc; In toluene; at 20 ℃; for 24h; Molecular sieve; Inert atmosphere;

With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 16h; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja4129394