{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid

Base Information

Chemical Name:{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid
CAS No.:1203505-83-2
Molecular Formula:C₂₄H₃₁NO₅S
Molecular Weight:445.58
Hs Code.:

Synonyms:{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid

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Chemical Property of {3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid

Chemical Property:

Purity/Quality:

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Technology Process of {3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid

There total 9 articles about {3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203503-64-3
{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-methoxy-phenyl}-acetic acid

: 1203505-83-2
{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid

Guidance literature:: With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 1203503-64-3
{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-methoxy-phenyl}-acetic acid

: 1203505-83-2
{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid

: 1203505-80-9
{3-[4-(2,2-Dimethyl-propionylamino)-2-(2-methyl-propane-2-sulfinylmethyl)-phenoxy]-4-methoxy-phenyl}-acetic acid

: 1203505-84-3
{3-[4-(2,2-Dimethyl-propionylamino)-2-(2-methyl-propane-2-sulfinylmethyl)-phenoxy]-4-hydroxy-phenyl}-acetic acid

: 1203505-81-0
{3-[4-(2,2-Dimethyl-propionylamino)-2-(2-methyl-propane-2-sulfonylmethyl)-phenoxy]-4-methoxy-phenyl}-acetic acid

Guidance literature:: With Uridine diphospho-D-glucuronic acid triammonium salt; β-nicotinamide adenine dinucleotide 2'-phosphate reduced tetra(cyclohexylammonium) salt; at 37 ℃; for 1h; pH=7.4; Product distribution / selectivity; Enzymatic reaction; phosphate buffer;

Reference yield:

: 1313757-49-1
methyl 2-(3-(2-bromomethyl-4-nitrophenoxy)-4-methoxyphenyl)acetate

: 1203505-83-2
{3-[2-tert-butylsulfanylmethyl-4-(2,2-dimethyl-propionylamino)-phenoxy]-4-hydroxy-phenyl}-acetic acid

: 1203505-80-9
{3-[4-(2,2-Dimethyl-propionylamino)-2-(2-methyl-propane-2-sulfinylmethyl)-phenoxy]-4-methoxy-phenyl}-acetic acid

: 1203505-84-3
{3-[4-(2,2-Dimethyl-propionylamino)-2-(2-methyl-propane-2-sulfinylmethyl)-phenoxy]-4-hydroxy-phenyl}-acetic acid

: 1203505-81-0
{3-[4-(2,2-Dimethyl-propionylamino)-2-(2-methyl-propane-2-sulfonylmethyl)-phenoxy]-4-methoxy-phenyl}-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 0 - 15 °C

2.1: N,N-Dimethylhydrazine / iron(III) chloride / methanol / 10 h / 65 °C

3.1: triethylamine / dichloromethane / 1 h / 15 - 40 °C

4.1: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 - 25 °C

4.2: 5 h / 10 - 20 °C / pH 2 - 3

5.1: β-nicotinamide adenine dinucleotide 2'-phosphate reduced tetra(cyclohexylammonium) salt; Uridine diphospho-D-glucuronic acid triammonium salt / 1 h / 37 °C / pH 7.4 / Enzymatic reaction; phosphate buffer

With Uridine diphospho-D-glucuronic acid triammonium salt; β-nicotinamide adenine dinucleotide 2'-phosphate reduced tetra(cyclohexylammonium) salt; water; sodium hydride; N,N-Dimethylhydrazine; triethylamine; sodium hydroxide; iron(III) chloride; In tetrahydrofuran; methanol; dichloromethane; mineral oil;