(2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol

Base Information

Chemical Name:(2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol
CAS No.:138925-00-5
Molecular Formula:C₃₄H₃₃NO₆
Molecular Weight:551.639
Hs Code.:

Synonyms:(2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol

Chemical Property:

Purity/Quality:

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Technology Process of (2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol

There total 3 articles about (2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138924-99-9
(2S,3R,4R)-1-O-Acetyl-5-N-phthalyl-2,3,4-tri-O-benzyladonitol

: 138925-00-5
(2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 25 ℃; for 16h;
DOI:10.1021/jo00030a014

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 138925-00-5
(2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol

Guidance literature:: Multi-step reaction with 2 steps

1: Ph₃P, diethyl azodicarboxylate / tetrahydrofuran / 1) 5 min, 0 deg C, 2) 12 h, 25 deg C

2: p-TsOH*H₂O / methanol / 16 h / 25 °C

With toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol;
DOI:10.1021/jo00030a014

Reference yield:

: 138481-57-9,138515-43-2,138515-46-5,139757-92-9,139757-93-0
(2S,3R,4R)-1-O-Acetyl-2,3,4-tri-O-benzyladonitol

: 138925-00-5
(2S,3R,4R)-2,3,4-Tri-O-benzyl-5-N-phthalyladonitol

Guidance literature:: Multi-step reaction with 2 steps

1: Ph₃P, diethyl azodicarboxylate / tetrahydrofuran / 1) 5 min, 0 deg C, 2) 12 h, 25 deg C

2: p-TsOH*H₂O / methanol / 16 h / 25 °C

With toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol;
DOI:10.1021/jo00030a014