1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose

Base Information

Chemical Name:1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose
CAS No.:1203651-64-2
Molecular Formula:C₃₄H₅₉NO₄Si₃
Molecular Weight:630.103
Hs Code.:

Synonyms:1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose

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Chemical Property of 1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose

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Technology Process of 1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose

There total 1 articles about 1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1203651-62-0
1β-(6-bromopyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose

: 98-80-6
phenylboronic acid

: 1203651-64-2
1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In toluene; at 100 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo902313g

Reference yield: 89.0%

: 1203651-64-2
1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose

: 1203651-69-7
1β-(6-phenylpyridin-2-yl)-1-deoxy-D-ribofuranose

Guidance literature:: 1β-(6-phenylpyridin-2-yl)-1-deoxy-2,3,5-tri-O-(t-butyldimethylsilyl)-D-ribofuranose; With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 40 ℃; for 48h;

With water; sodium hydrogencarbonate; pH=8;
DOI:10.1021/jo902313g