N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

Base Information

Chemical Name:N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine
CAS No.:1292221-11-4
Molecular Formula:C₄₈H₅₆N₆O₉
Molecular Weight:861.007
Hs Code.:

N<sub>1</sub>-(4-monomethoxytrityl)-N<sub>2</sub>,N<sub>3</sub>-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

Synonyms:N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

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Chemical Property of N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

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Technology Process of N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

There total 9 articles about N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1292221-10-3
N₁,N₄-bis(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

: 1292221-11-4
N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

Guidance literature:: N₁,N₄-bis(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.916667h;

With sodium carbonate; In dichloromethane; water;
DOI:10.1016/j.bmc.2011.01.061

Reference yield:

: 1292221-09-0
N₁,N₄-bis(tert-butoxycarbonyl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

: 1292221-11-4
N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 2.08 h / 0 - 20 °C

1.2: 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.92 h / 20 °C

With trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2011.01.061

Reference yield:

: 1292221-07-8
N₁,N₄-bis(tert-butoxycarbonyl)-N₂,N₃-bis(trifluoroacetyl)spermine

: 1292221-11-4
N₁-(4-monomethoxytrityl)-N₂,N₃-bis[2-(4-nitrophenyl)ethoxycarbonyl]spermine

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; sodium hydroxide / methanol

2.1: dmap / dichloromethane / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 2.08 h / 0 - 20 °C

3.2: 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.92 h / 20 °C

With dmap; water; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.01.061