Technology Process of 2-(3-(5-phenylthiophen-2-yl)naphthalen-2-yl)pyridine
There total 3 articles about 2-(3-(5-phenylthiophen-2-yl)naphthalen-2-yl)pyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate;
In
N,N-dimethyl acetamide;
at 140 ℃;
for 48h;
Inert atmosphere;
DOI:10.1021/ol400230y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; water; ethanol / 12 h / Inert atmosphere; Reflux
2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; silver hexafluoroantimonate / N,N-dimethyl acetamide / 48 h / 140 °C / Inert atmosphere
With
silver hexafluoroantimonate; tetrakis(triphenylphosphine) palladium(0); dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; sodium carbonate;
In
ethanol; N,N-dimethyl acetamide; water; toluene;
DOI:10.1021/ol400230y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; water; ethanol / 12 h / Inert atmosphere; Reflux
2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; silver hexafluoroantimonate / N,N-dimethyl acetamide / 48 h / 140 °C / Inert atmosphere
With
silver hexafluoroantimonate; tetrakis(triphenylphosphine) palladium(0); dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; sodium carbonate;
In
ethanol; N,N-dimethyl acetamide; water; toluene;
DOI:10.1021/ol400230y
