(2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol

Base Information

Chemical Name:(2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol
CAS No.:130444-50-7
Molecular Formula:C₁₉H₁₄ClO₃P
Molecular Weight:356.745
Hs Code.:

(2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ<sup>5</sup>-phospha-phenanthren-10-yl)-methanol

Synonyms:(2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol

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Technology Process of (2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol

There total 3 articles about (2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 35948-24-4
2-(2-hydroxyphenyl)-phenylphosphonous acid

: 89-98-5
2-chloro-benzaldehyde

: 130444-50-7
(2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol

Guidance literature:: In acetonitrile; at 80 ℃; for 3h;

Reference yield:

: 32186-92-8
6-Chloro-6H-dibenz<1,2>oxaphosphorin

: 130444-50-7
(2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / water / methanol / 1 h / Heating

2: 89 percent / acetonitrile / 3 h / 80 °C

With water; In methanol; acetonitrile;

Reference yield:

: 90-43-7,287950-96-3
2-Phenylphenol

: 130444-50-7
(2-Chloro-phenyl)-(10-oxo-10H-9-oxa-10λ⁵-phospha-phenanthren-10-yl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1) PCl₃ 2) ZnCl₂ / 1) a) 0.5h, 50 deg C b) 2.5h, 140 deg C 2) 5h, 140 to 210 deg C

2: 94 percent / water / methanol / 1 h / Heating

3: 89 percent / acetonitrile / 3 h / 80 °C

With water; zinc(II) chloride; phosphorus trichloride; In methanol; acetonitrile;