2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate

Base Information

• Chemical Name: 2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate
• CAS No.: 1487451-60-4
• Molecular Formula: C₁₈H₂₁F₃O₇SSi
• Molecular Weight: 466.507

Synonyms:2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate

Chemical Property of 2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate

There total 1 articles about 2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

phenyl-2,6-bis(acetoxymethyl)-4-bromotrifluoromethylsulphonate + trimethylsilylacetylene (1066-54-2) → 2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate (1487451-60-4)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; for 20h; Reflux;

DOI:10.1246/cl.150616

Reference yield: 46.6%

2,6-bis(acetoxymethyl)-4-(trimethylsilylethynyl)phenyl trifluoromethanesulfonate (1487451-60-4) + C17H25BO4 → C30H40O4Si

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 85 ℃; for 24h; Inert atmosphere;

DOI:10.1002/chir.23404

upstream raw materials:

trimethylsilylacetylene

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