phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside

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Chemical Name:phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside
CAS No.:1169827-75-1
Molecular Formula:C₃₈H₃₈O₅S₂
Molecular Weight:638.849
Hs Code.:

Synonyms:phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 45438-73-1
2-thenyl bromide

: 127299-77-8,130781-28-1,138181-68-7,130781-27-0
Phenyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 1169827-75-1
phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside

Guidance literature:: Phenyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

2-thenyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.018

Reference yield:

: 1169827-75-1
phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside

: 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-β-D-glucopyranose

: 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-α-D-glucopyranose

Guidance literature:: With N-iodo-succinimide; trifluoroacetic acid; In dichloromethane; water; at 0 ℃; for 2h; optical yield given as %de;
DOI:10.1016/j.tetasy.2009.02.018

Reference yield:

: 1169827-75-1
phenyl 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-1-thio-β-D-glucopyranoside

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-β-D-glucopyranosyl-(1->6)-[1:2,3:4]-di-O-isopropylidene-α-D-galactopyranoside

: 1169827-79-5
3,4,6-tri-O-benzyl-2-O-(thiophen-2-ylmethyl)-α-D-glucopyranosyl-(1->6)-[1:2,3:4]-di-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 3.5h; optical yield given as %de; stereoselective reaction;
DOI:10.1016/j.tetasy.2009.02.018