2-ethyl 2-diazoacetoacetate

Base Information

Chemical Name:2-ethyl 2-diazoacetoacetate
CAS No.:159050-44-9
Molecular Formula:C₁₅H₁₉N₃O₄
Molecular Weight:305.334
Hs Code.:

2-<N-(4-Methoxybenzyl)-N-methylamino>ethyl 2-diazoacetoacetate

Synonyms:2-ethyl 2-diazoacetoacetate

Suppliers and Price of 2-ethyl 2-diazoacetoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-ethyl 2-diazoacetoacetate

Chemical Property:

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Technology Process of 2-ethyl 2-diazoacetoacetate

There total 2 articles about 2-ethyl 2-diazoacetoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54527-70-7
2-[N-(4-methoxybenzyl)-N-methylamino]-ethyl acetoacetate

: 159050-44-9
2-ethyl 2-diazoacetoacetate

Guidance literature:: With triethylamine; Methanesulfonyl azide; In water; acetonitrile; for 12h; Yield given; Ambient temperature;
DOI:10.1021/jo00099a041

Reference yield:

: 151696-86-5
2-[(4-methoxy-benzyl)-methyl-amino]-ethanol

: 159050-44-9
2-ethyl 2-diazoacetoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1.) 0 deg C, 3 h, 2.) r.t., 1 h

2: MsN₃, Et₃N / acetonitrile; H₂O / 12 h / Ambient temperature

With triethylamine; Methanesulfonyl azide; In dichloromethane; water; acetonitrile;
DOI:10.1021/jo00099a041