benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside
CAS No.:329360-99-8
Molecular Formula:C₁₇H₂₂N₄O₅
Molecular Weight:362.385
Hs Code.:

Synonyms:benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside

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Technology Process of benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside

There total 4 articles about benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3396-11-0
cesium acetate

: Trifluoro-methanesulfonic acid (2R,3R,4S,5S,6S)-3-acetylamino-5-azido-2-benzyloxy-6-methyl-tetrahydro-pyran-4-yl ester

: 329360-99-8
benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside

Guidance literature:: With 18-crown-6 ether; In toluene; at 60 - 70 ℃; for 18h;
DOI:10.1016/S0957-4166(00)00452-3

Reference yield:

: 174151-46-3
benzyl 2-acetamido-2,3,4,6-tetradeoxy-α-L-threo-hex-3-enopyranoside

: 329360-99-8
benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / MCPBA; NaHCO₃ / CH₂Cl₂

2: 18 percent / NaN₃; NH₄Cl / dimethylformamide / 90 °C

3: pyridine / CH₂Cl₂ / -5 °C

4: 18-crown-6 / toluene / 18 h / 60 - 70 °C

With pyridine; sodium azide; 18-crown-6 ether; sodium hydrogencarbonate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0957-4166(00)00452-3

Reference yield:

: 329360-94-3
benzyl 2-acetamido-3,4-anhydro-2,6-dideoxy-α-L-talopyranoside

: 329360-99-8
benzyl 2-acetamido-3-O-acetyl-4-azido-2,4,6-trideoxy-α-L-altropyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 18 percent / NaN₃; NH₄Cl / dimethylformamide / 90 °C

2: pyridine / CH₂Cl₂ / -5 °C

3: 18-crown-6 / toluene / 18 h / 60 - 70 °C

With pyridine; sodium azide; 18-crown-6 ether; ammonium chloride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0957-4166(00)00452-3