C₆₈H₇₈F₃NO₁₆

Base Information

Chemical Name:C₆₈H₇₈F₃NO₁₆
CAS No.:1446004-02-9
Molecular Formula:C₆₈H₇₈F₃NO₁₆
Molecular Weight:1222.36
Hs Code.:

C<sub>68</sub>H<sub>78</sub>F<sub>3</sub>NO<sub>16</sub>

Synonyms:C₆₈H₇₈F₃NO₁₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₈H₇₈F₃NO₁₆

Chemical Property:

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Technology Process of C₆₈H₇₈F₃NO₁₆

There total 18 articles about C₆₈H₇₈F₃NO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374760-28-7
C₇₀H₈₃NO₁₇

: 407-25-0
trifluoroacetic anhydride

: 1446004-02-9
C₆₈H₇₈F₃NO₁₆

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 1446003-86-6
C₁₄H₂₆O₄Si

: 1446004-02-9
C₆₈H₇₈F₃NO₁₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 0.5 h / -20 °C / Inert atmosphere

2.1: bromine / dichloromethane / 0.67 h / Cooling with ice

2.2: 17 h / 20 °C / Inert atmosphere; Molecular sieve

2.3: 15 h / 20 °C

3.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

3.2: 2 h / 0 °C / Molecular sieve

4.1: methanol; sodium methylate / 2 h

5.1: triethylamine / acetonitrile / 1.33 h / 0 °C

6.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

6.2: 20 °C

7.1: tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.5 h / 20 °C

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; bromine; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;

Reference yield:

: C₁₆H₂₃NO₁₀

: 1446004-02-9
C₆₈H₇₈F₃NO₁₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / 20 °C

2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.2: 2 h / 0 °C / Molecular sieve

3.1: methanol; sodium methylate / 2 h

4.1: triethylamine / acetonitrile / 1.33 h / 0 °C

5.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

5.2: 20 °C

6.1: tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.5 h / 20 °C

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In methanol; dichloromethane; acetonitrile;