O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether

Base Information

Chemical Name:O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether
CAS No.:503306-51-2
Molecular Formula:C₇₉H₁₁₀O₁₃
Molecular Weight:1267.73
Hs Code.:

Synonyms:O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether

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Chemical Property of O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether

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Technology Process of O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether

There total 7 articles about O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183901-63-5
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

: 503306-43-2
2-hydroxyethyl 3,5-bis(octadecyloxy)benzyl ether

: 503306-51-2
O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/S0968-0896(02)00266-3

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 503306-51-2
O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether

Guidance literature:: Multi-step reaction with 6 steps

1.1: K₂CO₃ / dimethylformamide / 65 °C

1.2: 84 percent / dimethylformamide / 27 h / 65 °C

2.1: 100 percent / MeONa / CH₂Cl₂ / 14 h / 20 °C

3.1: 97 percent / LiAlH₄ / tetrahydrofuran / 12 h / 40 °C

4.1: 90 percent / CBr₄; Ph₃P / CH₂Cl₂ / 4 h / 20 °C

5.1: 73 percent / NaH / tetrahydrofuran / 72 h / Heating

6.1: TMSOTf / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 5.1: Williamson reaction;
DOI:10.1016/S0968-0896(02)00266-3

Reference yield:

: 112-89-0
1-Bromooctadecane

: 503306-51-2
O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl 3,5-bis(octadecyloxy)benzyl ether

Guidance literature:: Multi-step reaction with 6 steps

1.1: K₂CO₃ / dimethylformamide / 65 °C

1.2: 84 percent / dimethylformamide / 27 h / 65 °C

2.1: 100 percent / MeONa / CH₂Cl₂ / 14 h / 20 °C

3.1: 97 percent / LiAlH₄ / tetrahydrofuran / 12 h / 40 °C

4.1: 90 percent / CBr₄; Ph₃P / CH₂Cl₂ / 4 h / 20 °C

5.1: 73 percent / NaH / tetrahydrofuran / 72 h / Heating

6.1: TMSOTf / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 5.1: Williamson reaction;
DOI:10.1016/S0968-0896(02)00266-3